Coupling by heated capillary tube
The gases evolved by the sample are collected in the TGA furnace close to the crucible. They are quickly (approx. 100 ms) transferred to the ion source of the Mass Spectrometer thanks to the pressure difference between the TGA furnace (approx. 1 bar) and MS (approx. 10-7 mbar). The gases are not exposed to a temperature lower than 300 °C during the transfer. The ionized molecules and fragments are then separated according to their m/z ratio and detected.
The intensity of one or more selected characteristic m/z can be monitored and superimposed to the mass variation signal. Full spectra can also be acquired frequently over the duration of the TGA experiment. Mass spectrometers with amu ranges up to 300 can be employed.
Here the evolved gases are accelerated by a two steps pressure drop system. Their speed overcoming the speed of sound, they are instantaneously transferred to the ion source, avoiding any condensation or recombination during their route. Heavy, high boiling point molecules like metal vapors or polyaromatic compounds can thus be detected. Mass spectrometers with amu ranges up to 1024 can typically be employed.
– Features: best limit of detection, fast transfer time
– Benefits: applicable to small mass variations, easy to setup, detection of heavy molecules (with Supersonic System)
TGA-EGA and Simultaneous STA-EGA, from ambient to 1150°C or 1600°C THE HIGHLIGHTS Simplicity of use: thanks to both an ergonomic design and the dedicated market leading Calisto software, LABSYS evo is user friendly and intuitive to operate – LABSYS evo offers a “Plug & play” gas analyzer coupling device,enabling simultaneous MS, FTIR or GC/MS connections. […]
An innovative line of Thermal Analyzers (-120 / 830°C) with 3D-Inside technology: TG-DSC-EGA The HIGHLIGHTS Thermogravimetry Excellent TG signal baseline: the symmetry of the microbalance, with its sample and reference suspended vertically from the beam guarantee reproducible positioning of the sample over time and excellent stability of the TG signal baseline. Automatic compensation of Buoyancy: the sample […]
High-performance simultaneous TGA & DTA / DSC (ambient / 2400°C) with Evolved Gas Analysis The HIGHLIGHTS SETSYS Evolution is the standard for high performance TGA, TG-DSC and TG-DTA application. It is based on a complete modular thermal analysis platform for – TGA, DTA and DSC – Simultaneous TGA/DTA and TGA/DSC – The key to the […]
Large volume & high temperature TGA/STA-EGA (ambient to 2000°C) This is an extremely high performance weighing module used with the TGA 96. This balance can weigh samples up to 100 g and is well suited to measuring both micro-quantities of samples (a few milligrams) as well as large, dense samples while maintaining measurement resolution to […]
Stand-alone High Pressure Mass Spectrometer for gas composition analysis from 200 bar to 10-8 mtorr The RGAPro is a residual gas analyzer designed to work with the PCTPro-2000 or any other gas process for real-time compositional analysis of gas sorption and reaction processes. The system uses a 100 to 300 amu quadrupole mass spectrometer with […]